t-Butyl 4-bromopyridin-2-ylcarbamate
2-(Boc-amino)-4-bromopyridine
CAS: 207799-10-8
Molecular Formula: C10H13BrN2O2
t-Butyl 4-bromopyridin-2-ylcarbamate - Names and Identifiers
| Name | 2-(Boc-amino)-4-bromopyridine |
| Synonyms | 2-(Boc-amino)-4-bromopyridine t-Butyl 4-bromopyridin-2-ylcarbamate tert-Butyl 4-bromopyridin-2-ylcarbamate TERT-BUTYL 4-BROMOPYRIDIN-2-YLCARBAMATE ert-butylN-(4-bromopyridin-2-yl)carbamate tert-Butyl N-(4-bromo-2-pyridyl)carbamate tert-butyl N-(4-broMopyridin-2-yl)carbaMate (4-Bromo-pyridin-2-yl)-carbamic acid tert-butyl ester CarbaMicacid,N-(4-broMo-2-pyridinyl)-,1,1-diMethylethylester |
| CAS | 207799-10-8 |
| EINECS | 817-281-8 |
| InChI | InChI=1/C10H13BrN2O2/c1-10(2,3)15-9(14)13-8-6-7(11)4-5-12-8/h4-6H,1-3H3,(H,12,13,14) |
t-Butyl 4-bromopyridin-2-ylcarbamate - Physico-chemical Properties
| Molecular Formula | C10H13BrN2O2 |
| Molar Mass | 273.13 |
| Density | 1.453±0.06 g/cm3(Predicted) |
| Boling Point | 296.7±25.0 °C(Predicted) |
| Flash Point | 133.239°C |
| Vapor Presure | 0.001mmHg at 25°C |
| pKa | 11.89±0.70(Predicted) |
| Storage Condition | Keep in dark place,Inert atmosphere,2-8°C |
| Refractive Index | 1.573 |
t-Butyl 4-bromopyridin-2-ylcarbamate - Reference Information
| Use | tert-butyl (4-bromopyrimidin-2-yl) carbamate is useful as a pharmaceutical synthesis intermediate. |
| preparation | tert-butyl (4-bromopyrimidin-2-yl) carbamate can be prepared from 4-bromopyridin-2-amine, di-tert-butyl carbonate ((Boc)2O), 4-dimethylaminopyridine reaction, can be used for the preparation of ALD derivatives, for the treatment of EV71 and CAV16 infection and its caused by hand, foot and mouth disease and related complications. to a 250 ml round-bottom bottle was added 4-bromopyridin-2-amine (5g,28.90mmol), di-tert-butyl carbonate ((Boc)2O)(6.8g,31.16mmol), 4-dimethylaminopyridine (0.32g), tert-butanol (tert-Butanol)(70ml). Stir overnight at room temperature, concentrate in vacuo, and the resulting mixture is washed with 30ml hexane/ether in a volume ratio of 5:1 to give tert-butyl (4-bromopyrimidin-2-yl) carbamate (tert-butylN-(4-bromopyridin-2-yl)carbamate)(4.5g,57%) as a white solid. |
Last Update：2024-04-09 21:01:54
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